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Starch and oxidized starches of different molecular sises were carboxymethylated under identical conditions. The degree of substitution (DS) of the so obtained. CMS samples increases by decreasing the molecular sise of starch which, indeed, is a manifestation of higher extents of oxidation.
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FTIR and 1 HNMR spectra indicates that the hydroxyl groups of starches are substituted by carboxymethyl groups. Our work provides a simple method for highefficient preparation of CMS via ball milling in the presence of monochloro acetate and dichloroacetic acid and has great potential for broadening the application of starch.
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